4th WCSET-2015 at Japan

 

Applied Sciences and Engineering:

Title:           Analytical study of arsenic based herbo-mineral preparation Thalaka karuppu an Indian traditional medicine
Authors:      N. Kannan, S. Balaji, N. V. Anil Kumar
Abstract:     Thalaka karuppu (TK), is therapeutically used to treat various diseases like gonorrhea, epilepsy, syphilis, chronic fever, cancer, tuberculosis, asthma, psoriasis, and respiratory diseases, etc. This study was aimed to investigate the physicochemical fingerprint of commercially available arsenic based herbo-mineral preparation TK through various analytical techniques. The Uv-vis absorption peak at 288 nm corresponds to As (II). The formulation exhibits mixed nature of the arsenic compounds (AS (I), AS (II), AS (IV)). The vibrational spectroscopy peaks were observed at 802.23, 1033.77, 1404.08, 1643.24, 2368.42, 2854.45, 2923.88 and 3433.06 (cm-1) has good agreement with arsenic trioxide. The peaks at finger print region being assigned to 802.23 As-O and As-H (C-H bend) and 1033.77 (C-N stretching). The average grain size is found to be 30.11 nm using Scherrer formula. The XRD pattern observed sharp peak at 13.49 and 27.54 attributed to As2. The morphological investigation by SEM were observed irregular shaped (nearly spherical, elongated and interconnected structures) micro/nano sized particles. The selected portion of the spectrum reveals the presence of As (77.44 %), Pb (31.19 %) and Sn (-7.70 %) were evaluated through EDAX. The measured average diameter of the formulation was found to be 821.8 nm and width of 86.89 nm with % intensity of 100. The PDI of the formulation was 0.996. The formulation showed the zeta potential of -34.9. The spectral, structural and particle characterization analysis evident that the resulting morphologies, size diameter and their dispersity (colloidal stability) significantly helps in increase the efficacy of the formulation. Further in detailed in vitro and in vivo study is warranted to know the bioavailability and binding capacity of the TK formulation.

Keywords:   Thalaka Karuppu, Physicochemical Property, Analytical Study. Siddha, Nanoparticles
Pages:         054-055

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